N-Heptafluorobutyrylimidazole Basic information |
Product Name: | N-Heptafluorobutyrylimidazole |
Synonyms: | N-(HEPTAFLUORO-N-BUTYRYL)IMIDAZOLE;N-HEPTAFLUOROBUTANOYLIMIDAZOLE;N-HEPTAFLUOROBUTYRYLIMIDAZOLE;N-Heptafluorobutyryl-imidazole 98+;1-(Heptafluorobutyryl)imidazole, 98+%;2,2,3,3,4,4,4-Heptafluoro-1-(1H-imidazol-1-yl)butan-1-one, HFBI, 1-(Heptafluorobutyryl)-1H-imidazole;1-(Heptafluorobutyryl)imidazole [Acylating Agent];1-(Heptafluorobutyryl)-1H-imidazole |
CAS: | 32477-35-3 |
MF: | C7H3F7N2O |
MW: | 264.1 |
EINECS: | 251-063-8 |
Product Categories: | Acylation Reagent;Imidazol&Benzimidazole;Acylation (GC Derivatizing Reagents);Analytical Chemistry;GC Derivatizing Reagents;Acylation ReagentsBiochemicals and Reagents;Derivatization agentsBuilding Blocks;Analytical/Chromatography;Derivatization Reagents;Heterocyclic Building Blocks;Imidazoles;Luminescent Compounds/Detection;Aromatics;Intermediates & Fine Chemicals;Labeling and Diagnostics Reagents;Pharmaceuticals |
Mol File: | 32477-35-3.mol |
N-Heptafluorobutyrylimidazole Chemical Properties |
Melting point | 9-13 °C |
Boiling point | 161 °C(lit.) |
density | 1.490 g/mL at 25 °C(lit.) |
refractive index | n |
Fp | 171 °F |
storage temp. | 2-8°C |
solubility | Miscible with chloroform and methanol. |
pka | 1.37±0.10(Predicted) |
form | Oil |
color | Pale Yellow |
Sensitive | Hygroscopic |
BRN | 4488026 |
Stability: | Moisture Sensitive |
InChIKey | MSYHGYDAVLDKCE-UHFFFAOYSA-N |
CAS DataBase Reference | 32477-35-3(CAS DataBase Reference) |
NIST Chemistry Reference | N-Heptafluorobutyrylimidazole(32477-35-3) |
EPA Substance Registry System | 1-(Heptafluorobutyryl)imidazole (32477-35-3) |
Safety Information |
Hazard Codes | Xi |
Risk Statements | 36/37/38 |
Safety Statements | 26-36/37/39-24/25 |
RIDADR | NA 1993 / PGIII |
WGK Germany | 3 |
F | 3-10-21 |
Hazard Note | Irritant/Hygroscopic/Keep Cold |
HazardClass | IRRITANT, MOISTURE SENSITIVE, KEEP COLD |
HS Code | 29332900 |
MSDS Information |
Provider | Language |
---|---|
SigmaAldrich | English |
ALFA | English |
N-Heptafluorobutyrylimidazole Usage And Synthesis |
Chemical Properties | N-Heptafluorobutyrylimidazole is colorless liquid |
Uses | 1-(Heptafluorobutyryl)imidazole is used in gas chromatography for the determination of various pharmaceutical compounds like retronecine in biological matrixes. It acts as a reagent for derivatize amine-groups. It plays an essential role to reduce GC column degradation due to its non-acidic property. It is an acylating agent, which converts thermally unstable compounds to its more volatile derivative and then made suitable for GC analysis. |
Uses | N-Heptafluorobutyrylimidazole is a derivatization agent used in gas chromatography for determination of various pharmaceutical compounds such as retronecine in biological matrixes. |
General Description | May form a precipitate and may darken on storage-will not effect performance. |
Biochem/physiol Actions | Mild amine-group derivatizing reagent; non-acidic by-product prevents decomposition and reduces GC column degradation. |
N-Heptafluorobutyrylimidazole Preparation Products And Raw materials |
Raw materials | Chloroform-->1,1'-Carbonyldiimidazole-->Heptafluorobutyric acid-->Heptafluorobutyric anhydride-->Imidazole |
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