| 9-VINYLANTHRACENE Basic information |
| Product Name: | 9-VINYLANTHRACENE |
| Synonyms: | 9-Ethenyl anthracene;9-VINYLANTHRACENE;10-vinylanthracene;9-Ethenylanthracen;9-Vinylanthracene 97%;9-Vinylanthracene,97%;Anthracene, 9-ethenyl-;9-vinyl-anthracene radical cation |
| CAS: | 2444-68-0 |
| MF: | C16H12 |
| MW: | 204.27 |
| EINECS: | 219-486-2 |
| Product Categories: | Styrenes;Photoluminescent Materials > Fluorescent MonomersPolymer Science;Monomers;Photonic and Optical Materials;Styrene and Functionalized Styrene MonomersPolymer Science;Vinyl Halides, Amines, Amides, and Other Vinyl Monomers |
| Mol File: | 2444-68-0.mol |
| 9-VINYLANTHRACENE Chemical Properties |
| Melting point | 62-65 °C (lit.) |
| Boiling point | 61-66 °C/10 mmHg (lit.) |
| density | 1.1570 (estimate) |
| refractive index | 1.5000 (estimate) |
| Fp | 61-66°C/10mm |
| storage temp. | Store below +30°C. |
| form | powder to crystal |
| color | White to Yellow to Orange |
| BRN | 2041641 |
| CAS DataBase Reference | 2444-68-0(CAS DataBase Reference) |
| Safety Information |
| Safety Statements | 22-24/25 |
| WGK Germany | 3 |
| HS Code | 2902 90 00 |
| MSDS Information |
| Provider | Language |
|---|---|
| SigmaAldrich | English |
| ACROS | English |
| ALFA | English |
| 9-VINYLANTHRACENE Usage And Synthesis |
| Chemical Properties | yellow to green crystalline solid |
| Uses | 9-Vinylanthracene (cas# 2444-68-0) is a compound useful in organic synthesis. |
| Synthesis Reference(s) | The Journal of Organic Chemistry, 56, p. 4035, 1991 DOI: 10.1021/jo00012a043Synthesis, p. 319, 1981 |
| Purification Methods | Purify it by vacuum sublimation. It has also been purified by chromatography on silica gel with cyclohexane as eluent, and recrystallised from EtOH [Werst et al. J Am Chem Soc 109 32 1987]. [Beilstein 5 IV 2415.] |
| 9-VINYLANTHRACENE Preparation Products And Raw materials |
| Raw materials | Ethanol-->Methanol-->Tetrahydrofuran-->Acetic acid-->N,N-Dimethylformamide-->Phosphorus oxychloride-->Aluminum chloride-->Sodium borohydride-->Iodomethane-->p-Toluenesulfonic acid-->Acetyl chloride-->Sodium acetate-->Sodium azide-->Triphenylphosphine-->Tosyl chloride-->Oxalyl chloride-->Potassium tert-butoxide-->1,2-Dichloroethane-->Anisole-->1,2-Dichlorobenzene-->Methyl bromide-->Potassium bisulfate-->Anthracene-->DBU-->2-Pyrrolidinone-->Anthrone-->3-Chloro-1-propanol-->Vinylmagnesium bromide-->9-Anthraldehyde |
| Preparation Products | polyvinyl anthracene |
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