3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE
3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE
  • CAS No.:5439-14-5
Other grades of this product :
3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE Basic information
Product Name:3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE
Synonyms:LABOTEST-BB LT00847264;ACID CAPTOR H;Dihydropyridopyrimidinone;3,4-DIHYDRO-2-PYRIDOL[1,2-A]PYRIMIDINONE;3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE;2H-Pyrido[1,2-a]pyrimidin-2-one,3,4-dihydro-;3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE 98+%;3,4-dihydropyrido[1,2-a]pyrimidin-2-one
CAS:5439-14-5
MF:C8H8N2O
MW:148.16
EINECS:226-618-2
Product Categories:Condensation & Active Esterification;Synthetic Organic Chemistry;Esterification ReagentsBuilding Blocks;Alkylation Reagents;Derivatization Reagents;Heterocyclic Building Blocks;Pyrimidines
Mol File:5439-14-5.mol
3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE Chemical Properties
Melting point 185-187 °C
Boiling point 271℃
density 1.26
Fp 118℃
storage temp. Sealed in dry,Room Temperature
solubility Chloroform (Sparingly), Methanol (Slightly)
form Solid
color Light Yellow
BRN 3667723
Safety Information
Safety Statements 22-24/25
WGK Germany 3
9-23
HS Code 29339900
MSDS Information
ProviderLanguage
SigmaAldrich English
3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE Usage And Synthesis
Purification MethodsDissolve it in CHCl3, filter, evaporate, then recrystallise the residue from EtOH/Me2CO (needles) which can be washed with Et2O and dried. It can also be recrystallised from CHCl3/pet ether or CHCl3/hexane. The hydrochloride has m 295-295o (dec, from EtOH or MeOH/Et2O), the hydrobromide has m 299-300o(dec) (from MeOH/Et2O) and the picrate has m 224-226o(corr), m 219-220o from EtOH. [Adams & Pachter J Am Chem Soc 74 4906 1952, Lappin J Org Chem 23 1358 1958, Hurd & Hayao J Am Chem Soc 77 115 1955, Beilstein 24 III/IV 299.]
3,4-DIHYDRO-2H-PYRIDO[1,2-A]PYRIMIDIN-2-ONE Preparation Products And Raw materials

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